By Andreis Kulicke
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Thus, recording the spectra under scalar low power decoupling yields characterization information and some dynamic measurements, concerning Tv T2 (line widths) and nuclear Overhauser enhancement (NOE) for lightly crosslinked polymers. 1 Characterization of Polymer Networks The linewidths in the l 3 C NMR spectra of swollen chloromethylated polystyrene and poly[styrene-co-(chloromethyl)styrene] [P(S-co-ClS)] crosslinked with divinylbenzene (DVB) are sensitive to the degree of crosslinking. Although all the networks have the same nominal degree of crosslinking (1-2 wt.
Likewise, a deviation in the temperature dependence of Ea from the Arrhenius law (inflection) is ascribed to the presence of two xcs for rapid and slow segments, respectively. 2 kJ/mole) 103) . Spin-spin relaxation and broad line NMR studies of the curing of unsaturated polyesters with styrene, reveal the existence of three T2 relaxation times, although the shortest T2 is not directly observed. However, from the loss of initial magnetization, 1(0), during the crosslinking process the fraction of the three types of protons could be estimated (Fig.
Andreis and J. L. Koenig 116 In the case of extreme narrowing, (coc + coHxc
Advances in Polymer Science 89 by Andreis Kulicke