By A. R. & Boulton, A. J. [Eds]. Katritzky
(from preface)Volume thirteen of this serial booklet contains six chapters of which 4 care for basic debts of compound sessions: 1-azirines (F. W. Fowler), phenanthridincs (B. R. T. Keene and P. Tissington), tri-thiapentalenes (N. Lozac'h), and heterocyclic fcrrocenes (F. D. Popp and E. B. Moynahan). the opposite chapters are involved in specific facets of the chemistry of teams of heterocycles: the tautomerism of purines (B. Pullman and A. Pullman) and quantitative points of the electrophilic substitution reactions of five-membercd earrings (G. Marino).
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98 Ferrocenecarboxaldehyde also reacts with barbituric acid t o give 99,07 with 1,2dimethylpyridinium iodide t o give with a series of substituted M. Furdik, S. Torna, and J. Suchy, Chem. Zwesti 17, 21 (1963);Chem. Abstr. 59, 10116 (1963). 93 J. W. Cusic and P. S. Patent 3,395,144 (1968); Chem. Abstr. 69, 92 964605. (1968). F. D. Popp and E. B. Moynahan, J . Med. Chem. 13, 1020 (1970). 95 J. Tirouflet arid J. Boichard, C. R. Acad. Sci. 250, 1861 (1960). 96 J. Boichard, J. Monin, and J. Tirouflet, Bull.
34, 1974 (1969). 132 34 F. D. POPP AND E. B. MOYNAHAN e Fa Fa [Sec. C. Fk F e r r o ~ e n e ,ferrocene~arboxaldehyde,~~' ~~~ and hydroxymethylhave all been used to prepare various and hydro~yethylferrocene~~~ ferrocenylcarbohydrates. Ferrocenecarboxylic acid chloride and 1,3O-methylenegly~erol~~~* 140 gave the ferrocenecarboxylate (163). W. Treibs, Nuturwissenschuften 52, 496 (1965). N. DeBelder, E. J. Bourne, and J. B. Chem. 5486 (1964). N. DeBelder, E. J. Bourne, and J. B. Pridham, J . Soc. 4464 (1961).
S. Lisitsyna, and M. R. Shemtova, Dokl. Akad. Nauk SSSR 130, 341 (1960); Chem. Abstr. 54, 10986 (1960). l o 2 I. K. Barben, J . Chem. 1827 (1961). 1°3 M. Shiga, H. Kono, I. Motoyama, and K. Hata, Bull. Chem. SOC. Japan 41, 1897 (1968). 1°4 F. D. Popp, Adwan. HeterocycE. Chem. 9, 1 (1968). 101 A. Sec. ~~ of 106 with manganese dioxide gave the corresponding ketone. 7 6 R O S-N I -cHbpo e Fe 0 II OC-Ph OH I -CH- e Reaction of the quaternary ammonium compound 107 with piperidine,lo5 p y r r ~ l i d i n e , ~ ~and ~ - "potassium ~ phthalirnidelo5 gave compounds ofthe type 108-110.
Advances in Heterocyclic Chemistry, Vol. 13 by A. R. & Boulton, A. J. [Eds]. Katritzky